5-Butyl-5-ethylbarbituric acid: a phase transition at low temperature

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5-Butyl-5-ethylbarbituric acid: a phase transition at low temperature.

The room-temperature crystal structure of 5-butyl-5-ethylbarbituric acid (generally known as butobarbitone), C10H16N2O3, was reported in space group C2/c [Bideau (1971). C. R. Acad. Sci. Paris Ser. C, 272, 757-760]. A redetermination at 120 K using synchrotron radiation shows the space group at this temperature to be P2(1)/n and not C2/c. There are two crystallographically independent molecules...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section C Crystal Structure Communications

سال: 2005

ISSN: 0108-2701

DOI: 10.1107/s0108270105008486